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Facilities
Equipment
for characterization of optical films
- transmission
null ellipsometry
To
study optical anisotropy of LC layers and
functional films, 3D orientational molecular ordering in the films, we
actively
use transmission null ellepsometry (TNE) technique based on Senarmont
method.
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The
optical scheme of this method is presented below.
The probe beam (628 nm) linearly
polarized
at 45° with respect to vertical line is directed to anisotropic
sample. The
sample is oriented so that its x or y in-plane axis is vertical.
Passing the
sample, the testing beam becomes elliptically polarized. The elliptical
polarization is transformed back to linear by a quarter wave plate with
a slow axis
parallel to that of the polarizer. The angle ϕ
of output polarization, determined by rotation of a
linear analyzer, gives the in-plane retardation (ny-nx)d.
Then the sample is
rotated around the x axis vertically aligned and the polarization
angle ϕ
is measured as a function of the incidence angle θ.
The out-of-plane retardation (nz-nx)d
is determined
by fitting a theoretical expression of ϕ(θ).
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Scheme of null ellipsometry setup
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Photograph of null ellipsometry setup |
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